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为研究钛合金轮盘内部硬α夹杂疲劳裂纹扩展特性,对含预置硬α夹杂钛合金轮盘开展低循环疲劳裂纹扩展试验。结果表明:5229次循环后轮盘破裂;疲劳断口宏观、微观特征显示,预置硬α夹杂为本次疲劳破坏的疲劳源;在裂纹扩展前期,轮盘断口裂纹扩展速率较材料试验数据快;在裂纹扩展中期,断口裂纹扩展速率曲线呈对数线性关系;为了解决疲劳裂纹扩展后期疲劳条带不易识别的问题,使用等效裂纹扩展模型拟合断口裂纹扩展速率曲线,从而可以利用疲劳条带宽度来计算总寿命。同时,利用断口数据,提出和总结了预置硬α夹杂钛合金轮盘裂纹扩展特性仿真研究的方法。仿真研究显示:基于Paris公式建立裂纹扩展模型能较好地预测轮盘裂纹扩展特性;轮盘由于疲劳发生最终断裂破坏时,裂纹前沿的应力强度因子远大于断裂韧性,因此,不宜使用应力强度因子直接作为破裂准则。 相似文献
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Xiaoqing Si Jian Cao Sheng Liu Xiaoguo Song Junlei Qi Yongxian Huang Jicai Feng 《International Journal of Hydrogen Energy》2018,43(5):2977-2989
A novel low-temperature sealing method was developed to seal solid oxide fuel cells. The 3D Ni nanosheet array was pre-fabricated on faying surfaces of Crofer22APU interconnect and NiO-YSZ anode-support. Then it was covered with Au film without changing its morphology. This special nanostructure improved sintering efficiency between Ag nanoparticles and substrates. A dense joint was obtained at the low-temperature between 250 °C–300 °C. This method effectively avoided the oxidation of interconnect during sealing. When joints were sealed at 300 °C, the shear strength reached 16 MPa. The fracture was mainly located in the central Ag layer, presenting a significant plastic deformation. Due to the effective protection of Ni layer, joints also possessed excellent oxidation resistance in oxidizing atmosphere at 800 °C for 400 h. After high-temperature oxidation, the shear strength was increased to 23 MPa, revealing an increasement of 43.8% compared with the as-sealed condition (16 MPa). This sealing method has great potential in sealing solid oxide fuel cells. It also can be extended to seal other energy-conversion devices. 相似文献
54.
通过矿物浮选试验、动电位测定以及吸附量测试,考察了4种淀粉抑制剂对赤铁矿和石英浮选性能的影响,并探讨了其作用机理。在碱性条件下,改性淀粉抑制剂对赤铁矿抑制效果明显,且以改性玉米淀粉效果最佳,改性磷酸酯淀粉、改性羧甲基淀粉的抑制效果次之,而普通淀粉抑制作用一般。同时4种淀粉抑制剂对主要脉石矿物石英的抑制效果均不明显。pH=10~12.5条件下,改性玉米淀粉因其羟基氧和裸露在赤铁矿表面的铁元素发生了化学键合,因而选择性抑制能力最佳。分子动力学模拟表明,改性玉米淀粉片段与赤铁矿作用更为紧密,验证了改性淀粉能更好地抑制赤铁矿。 相似文献
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Yuanfang Tao Xin Ji Dr. Jian Zhang Yue Jin Nannan Wang Prof. Yubing Si Prof. Weili Zhao 《Chembiochem : a European journal of chemical biology》2020,21(21):3131-3136
Near-infrared (NIR) fluorescent probes are very significant for detecting cysteine in biological systems. Herein, we report a highly selective and sensitive NIR turn-on fluorescent probe (BDP-NIR) based on BODIPY with large Stokes shift (105 nm) for detecting Cys. We clarified the sensing mechanism based on the different thiol-induced SNAr substitution/rearrangement reaction of the probe with cysteine and homocysteine/glutathione, which leads to the corresponding amino- and thiol-BODIPY dyes with distinct photophysical properties. Moreover, a novel mechanism of fluorescence quenching was demonstrated by density functional theory calculation. The reason for the fluorescence quenching of the probe might be intersystem crossing (from singlet to triplet excited state). Moreover, BDP-NIR had a high linear dynamic range of 0–500 μM, which was promising for detecting cysteine quantificationally. Significantly, BDP-NIR was capable of sensing endogenous cysteine in living cells and in vivo. 相似文献
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Meimei Xia Jian Chen Xiao‐Jun Zeng 《International Transactions in Operational Research》2020,27(2):1080-1100
Existing approaches to data envelopment analysis focus mainly on the derivation of the efficiency of the individual decision‐making unit (DMU) or on the calculation of the weights of multiple inputs or outputs, but pay little attention to the team interest of all the DMUs. Motivated by the idea of team reasoning, in which the benefit of the team is of higher importance than that of each individual, this paper considers all the DMUs as a team and introduces the team indexes including the overall efficiencies, variance, boundaries of all the DMUs, and relationships between DMUs. Several models are first developed to estimate values of the team indexes based on which decision makers can provide their preferences regarding them. Then, models are established to obtain the interval efficiencies of individual DMUs under the condition that the team indexes are satisfied. Several examples are given to illustrate the proposed approaches and verify their applicability. 相似文献
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